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The efficient synthesis of orthogonally protected glycerols, 2-aminopropane-1,3-diols and 2aminobutane-1,4-diols that can constitute useful tools in heterocyclic chemistry, is reported. These interesting tri-functionalized small synthons were easily prepared from serine or aspartic acid. In addition, these substrates can be readily transformed into their iodide derivatives in very good yields.

Orthogonally protected glycerols and 2-aminodiols, useful building blocks in heterocyclic chemistry