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A new efficient method was developed for the preparation of 2-methyl-1-(2-morpholinoethyl)- 1H-indole-3-carboxylic acid. The new method involves N-alkylation of 7-methoxy-2- methylindole with 4-(2-chloroethyl)morpholine hydrochloride followed by trichloroacetylation and hydrolysis in 3 steps and 88% overall yield.

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Improved procedure for the preparation of 7-methoxy-2-methyl-1-(2-morpholinoethyl)-1H-indole-3-carboxylic acid, key intermediate in the synthesis of novel 3-amidoindole and indolopyridone cannabinoid ligands