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The (+)and (–)-enantiomers of tricarbonyl[methyl (2E,4E)-6-oxo-2,4-hexadienoate]iron are prepared in 4 steps from commercially available hexadienal (26% and 25% yields, respectively).

A shortened synthesis of optically pure tricarbonyl(methyl 6-oxo-2,4-hexadienoate)iron leading to improved yield