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A series of new 2,5-disubstituted-1,3,4-oxadiazoles derived from benzo[b]thiophene was obtained by dehydrative cyclization of the corresponding N,N’-diacylhydrazines, in presence of an excess of phosphorous oxychloride. The structures of the new synthesized compounds were confirmed by spectral analysis.

New non-symmetrical 2,5-disubstituted-1,3,4-oxadiazoles bearing a benzo[b]thiophene moiety