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New diazapolyoxa macrocyclic ditosylates with 17–28-membered rings were synthesized by the application of the RCM technique to suitable α,ω-dienes. These compounds were employed as neutral carriers in Li-selective electrodes. The electrodes exhibited nearly Nernstian responses with relatively high selectivity for lithium over other inorganic cations.

Synthesis of azacrown sulfonamides via ring closing metathesis and their evaluation in lithium ion selective electrodes