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5-(R,S)-3H-1,2-dithiol-3-one derivatives with R=butyl, ethyl, phenyl, cyclopentyl, octyl, pchlorophenyl, p-bromophenyl and p-methoxyphenyl were prepared in moderate to good yield from the reaction of the corresponding 5-(R,S)-3H-1,2-dithiol-3-thione with Hg(CH3COO)2 in glacial acetic acid.

Synthesis of 5-(alkylthio or arylthio)-3H-1,2-dithiol-3-one derivatives