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A method for the synthesis of thiazapodands from 4'-formylbenzothiacrown ethers was developed. It involves nucleophilic regioselective cleavage of the macrocycle by heating with MeNH2 and MeNH3 + Cl - .

Macrocycle opening in crown ethers. Synthesis of thiazapodands from 4'-formylbenzothiacrown ethers