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Various 2,3-dihydro-2-substituted-2-vinyl-1,4-benzodioxins 6 are obtained by alkylation of the methyl carbonate of 2,3-dihydro-1,4-benzodioxin-2-ylideneethanol 5 with various carbon nucleophiles in the presence of a palladium complex. Altough the yields in alkytion products are good in the case of a non-bulky nucleophile, formation of the diene 7 was generally observed when a bulky nucleophile was used.

Palladium–catalyzed synthesis of 2,3-dihydro-2-substituted-2-vinyl-1,4-benzodioxins