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We synthesized a new hybrid organo-inorganic polyoxometalate from Na2WO4 and di-sodium salt of para-nitrophenyl ester of phosphoric acid, Na2C6H4NO2@[PW12O40]. Photochemical activity of the compound towards mandelic acid and isopropyl alcohol was studied. It was shown that the polyoxometalate synthesized behaves itself as a powerful photooxidazing agent and/or a catalyst of the photochemical oxidation of the said H-atom donors by nitrocompound in the presence of oxygen.

SYNTHESIS AND PHOTOCHEMICAL PROPERTIES OF POLYOXOMETALATES CONTAINING <i>para</i> – NITROBENZENE PHOSPHOROUS ACID FRAGMENT