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Transition-metal chalcogenide compounds with facile preparation and multifunctional elements act as ideal photothermal agents for cancer theranostics. This work synthesizes Cu 7.2 S 4 /5MoS 2  composite nanoflowers and investigates the crystal growth mechanism to optimize the synthesis strategy and obtain excellent photothermal therapy agents. Cu 7.2 S 4 /5MoS 2  exhibits a high photothermal conversion efficiency of 58.7% and acts as a theranostic nanoplatform and demonstrated an effective photothermal–chemodynamic–photodynamic synergetic therapeutic effect in both  in vitro  and  in vivo  tests. Moreover, Cu 7.2 S 4 /5MoS 2  shows strong photoacoustic signal amplitudes and computed tomographic contrast enhancement  in vivo . These results suggest a potential application of Cu 7.2 S 4 /5MoS 2  composite nanoflowers as photo/H 2 O 2 -responsive therapeutic agents against tumors.

A Near-Infrared Light Triggered Composite Nanoplatform for Synergetic Therapy and Multimodal Tumor Imaging