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The synthesis and characterization of organoantimony(III) compounds of type 2(Ph2E)C6H4SbPh2 (E = P, As, Sb) was mainly promoted by their prospective use as soft bidentate chelating ligands in the coordination chemistry of late transition metals. The mass spectra and elemental analysis data for the related bismuthane 2-(Ph2Sb)C6H4BiPh2 were also reported. In the last decade, compounds with Lewis acidic functional groups containing antimony were shown to have applications in anion or molecular sensing, and catalysis. We report an alternative method with fewer steps and better yield for the synthesis for (2bromophenyl)diphenylstibane, 2-BrC6H4SbPh2 (1) and the serendipitous formation of the {2′-bromo-

Molecular structures of (2-bromophenyl)diphenylstibane and {2’-bromo-[1,1’-biphenyl]-2yl}diphenylstibane