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NiO–LSGM reactivity during sintering at high temperatures in air leads to the formation of LaNiO 3 -type phase which is found to be insulating for oxygen ions. XRD analysis of the NiO-LSGM samples after sintering at 1350 °C in air showed cubic (Pm-3m) LaNiO 3 -based phase with a lattice parameter of 3.856 Å in addition to the cubic structure of LSGM20-17. STEM/EDX analysis of the NiO– LSGM interface showed the presence of a Ni-containing perovskite phase (La, Sr) (Ga, Ni, Mg)O 3 – x   in the diffusion layer of LSGM. The probable composition of the LaNiO 3 - type phase that formed during sintering is discussed.

XRD and TEM study of NiO–LSGM reactivity