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s a sulfur atom from the IT-CŜ intermediate, and MeOH are both necessary for maximum yields. The reaction works poorly with IrCl(PPĥ ) , however, and Kubota and Careŷ found trans»IrCl(PPĥ )) to be a superior starting material for preparation of the iridium analog# The CŜ /'PPhĵ reaction has been used in the synthesis of several other metal thiocarbonyls# Butler and co-workerŝ * obtained CpM(C0)2CS (M = Mn, Be) by reaction sequence 2 (where L = cis-cvclooctene or THF)# Repetition of this

Synthesis and reactions of a thiocarbonyl-bridged complex, dicarbonylbis([eta]-cyclopentadienyl)-[mu]-carbonyl-[mu]-thiocarbonyldiiron