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X-ray diffraction (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), UV-vis diffuse reflectance spectroscopy (DRS), Fourier transform infrared spectra (FT-IR), etc. The composite formed by the chemical method exhibited obviously better photocatalytic activity than the mechanical mixing sample under visible light irradiation. The possible mechanism for the enhanced catalytic efficiency may be due to the synergistic effect between the WO and g-C N tighter interface and the improved optical absorption in visible 3 3 4

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In situ preparation of WO3/g-C3N4 composite and its enhanced photocatalytic ability, a comparative study on the preparation methods of chemical composite and mechanical mixing