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Hexagonal spindle-shaped mesoporous alumina was prepared using Al-based metal-organic frameworks (MOFs) MIL-96 as precursor through thermal treatment method. The MIL-96 and alumina products were characterized by XRD, SEM, BET and 27Al-NMR. Results from these characterizations showed that alumina products keep the morphology of their precursor, and the thermal treatment time has large effect on the alumina microstructures. In addition, the aluminium environment and the ratio of Al (IV)/Al (V)/Al (VI) could also be modulated by the treatment time.

The Transformation of Al-based MOFs to Mesoporous Al2O3 with Pre-defined Morphology and Modulated Microstructure