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Translation of new methodologies for labeling nonactivated aromatic molecules with (18)F remains a challenge. Here, we report a one-step, regioselective, metal-free (18)F-labeling method that uses a hypervalent iodonium(III) ylide precursor, to prepare the radiopharmaceutical (18)F-3-fluoro-5-[(pyridin-3-yl)ethynyl]benzonitrile ((18)F-FPEB).

Iodonium Ylide–Mediated Radiofluorination of 18F-FPEB and Validation for Human Use

Iodonium Ylide–Mediated Radiofluorination of ¹⁸F-FPEB and Validation for Human Use