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The Pentane- and Toluene-Soluble Fractions of a Petroleum Residue and three Coal Tars by Size Exclusion Chromatography and UV-Fluorescence Spectroscopy — A petroleum atmospheric pressure distillate residue and three tars derived from different coals using different severities of thermal treatment were separated into seven fractions using column chromatography on silica and sequential elution by the solvent sequence pentane, toluene, acetonitrile, pyridine, 1-methyl-2-pyrrolidinone (NMP) and water. The fractions from the four extractions have been compared using size exclusion chromatography (SEC) in NMP as eluent and by synchronous ultra-violet-fluorescence (UV-F). This paper concerns the pentane and toluene soluble fractions only since these are the least polar fractions.

oil and gas science and technology

The Pentane- and Toluene-Soluble Fractions of a Petroleum Residue and three Coal Tars by Size Exclusion Chromatography and UV-Fluorescence Spectroscopy