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Amorphous alloy powder of 57at%Ti-Cu is prepared by the mechanical alloying of the elemental Ti and Cu powders by using a Spex Mixer/Mill Model 8000. The amorphization reaction is monitored by X-ray diffraction, scanning electron microscopy and differential thermo analysis. During the milling a layered structure of the crystalline elements is developed. These layers become thinner and the amorphous parts grow, when the alloying period is increasing. The X-ray diffraction patterns begin to show broad peaks from the MA period of 36ks. The crystallization temperature of CuTi is presumed around 650K from the results of DTA and X-ray diffraction.

Amorphous Formation of 57at%Ti-Cu Mixed Powders by Mechanical Alloying and Its Crystallization.