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A mild, versatile and efficient method to form biaryl sultams through silver-catalyzed intramolecular oxidative decarboxylative C-H arylation reactions has been developed. The present protocol features a broad substrate scope and very good tolerance to different substituent groups with satisfactory yields, giving access to a wide range of biaryl sultam derivatives. S O O N Ag2SO4 (10 mol%) K2S2O8 (2 equiv) CH3CN, 100 oC, 12 h S O O

Silver-catalyzed intramolecular oxidative decarboxylative C-H arylation reactions for synthesis of biaryl sultams