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This paper describes preparation of the two-types of cations composed of di(1-azulenyl)methylium units based on a new structural principle of cyanine–cyanine (C–C) hybrid for the design of polyelectrochromic materials. Voltammetric analysis of these cations revealed the idealized reversible two-step, two-electron redox properties. Two-step color changes presumed by their C–C hybrid structure were revealed by their electrochemical reduction. The scope of the creation of the stabilized polyelectrochromic materials taking the new structural principle with azulene skeletons is demonstrated by two-types of examples.

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Cyanine–cyanine hybrid structure as a stabilized polyelectrochromic system: synthesis, stabilities, and redox behavior of di(1-azulenyl)methylium units connected with electron-accepting π-electron systems