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reaction to form the compound MnBi occurs at 715゚K. The conventional alloying procedure of the compound MnBi was to keep a mixture of manganese and bismuth just below the peritectic temperature. However, the reaction in the present method is found not to proceed effectively except for the initial stage of the reaction. Hence, in this case the magnetic separation technique is usually applied and the final yield of the bonded compound MnBi by the above-mentioned procedure is about 90 per cent(5). The present author made an attempt to expedite the reaction by solid diffusion just below the eutectic temperature. Electrolytic manganese and bismuth of high purity were ground into fine powders, mixed in equi-atomic ratio, pressed at about 2t/cm2 to mold into small lumps and kept for a specified time just below 535゚K in an evacuated hard glass capsule. Then the solid reaction between the two ingredients proceeded, and the reaction

Preparation of Manganise Bismuthide by the Solid Diffusion Method and Its Thermal and Magnetic Properties