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Glass formation was achieved by mechanical milling of crystalline Ni 59 Ti 16 Zr 20 Sn 5 pre-alloyed powders. Compared to the glassy alloy ribbon of the same composition obtained by melting-spinning method, the alloy powders milled for 24h exhibited a lower crystallization temperature and do not have a distinct glass-transition characteristic. X-ray diffraction (XRD) and transmission electron microscopy (TEM) results indicated that a small fraction of the powder exists in nanocrystalline state within the glassy matrix. The obtained Ni 59 Ti 16 Zr 20 Sn 5 powdered specimen was heated rapidly by microwave radiation and the bulk porous sample was obtained under a low applied pressure of 5 MPa.

Glass Formation in a Ni-Based Multicomponent Alloy by Mechanical Milling and Microwave Treatment of The Obtained Powders