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New hydrides of Mg–TM–H systems, where TM = Zr, Nb and Mo, have been prepared by using cubic-anvil-type apparatus, and their crystal structure and hydrogen content have been investigated. The high-pressure synthesis was performed at 1073–1173 K under 2–5 GPa. In the Mg–Zr–H system, a new hydride Mg2Zr3Hy with a monoclinic structure (a ¼ 0:8591ð1Þ nm, b ¼ 0:33539ð5Þ nm, c ¼ 0:5816ð1Þ nm,  ¼ 103:06ð3Þ  ) was obtained by exposing a mixture of MgH2 and ZrH2 to pressure of 2 to 5 GPa at 1073 K for 2 h. In the Mg–Mo system, a new hydride Mg3MoH6 was synthesized by exposing a mixture of MgH2 and Mo to 5 GPa at 1173 K for 2 h. The hydride was found to have a hexagonal structure (a ¼ 0:49958ð6Þ nm, c ¼ 0:8840ð2Þ nm). In the Mg–Nb–H system, a new hydride Mg4NbHy was also synthesized by exposing a mixture of MgH2 and Nb to 5 GPa at 1073 K for 2 h.

High-Pressure Synthesis of Novel Hydrides in Mg&ndash;TM Systems (TM = Zr, Nb and Mo)

High-Pressure Synthesis of Novel Hydrides in Mg–TM Systems (TM = Zr, Nb and Mo)