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Alcohols and phenols were tetrahydropyranylated in the presence of  H7[PMo8V4O40] in good to excellent yields in acetonitrile and under  solventfree reaction conditions. A mild and convenient method for the  formation and deprotection of tetrahydropyranyl ethers (THP ethers) is  described. The formation of THP ethers from the corresponding alcohols was  accomplished in the presence of acid-sensitive functional groups

Catalytic tetrahydropyranylation of phenols and alcohols using vanadium(V)-substituted polyoxomolybdates