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New mononuclear (Cu2(L1)2(H2O))2H2OCH3OH) (cyCu)2, multinuclear (Cu2(L1)2K2)(Ni(CN)4) (cy- CuKNi), and dinuclear Ni(L1)Lu(NO3)3 (cyLuNi), Cu(L1)Lu(NO3)3 (cyLuCu) and Zn(L1)Lu((NO3)2CH3COO)CH3OH (cyLuZn) complexes incorporating chiral Schiff base ligands were prepared and characterized by various techniques such as solid-state CD spectra, diffuse reflectance electronic spectra, IR spectra, and single crystal X-ray diffraction analysis. Crystal structures were also compared with previous ones, namely (Cu(L2))(H2O) (diCu), Cu(L1)Gd(NO3)3 (cyGdCu). Interestingly, determined crystal structures exhibited drastically different structural characteristics as regards coordination numbers, crystalline solvents, features and strain condition, nevertheless with little modification in 3d metal substitution and/or modified organic ligands. In this paper, comparison of common components of structures will be discussed sys- tematically.

Variety of Crystal Structures of Chiral Schiff Base Lu(III)-Ni(II)/ Cu(II)/Zn(II) and the Related Complexes