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A series of mono protected ,-diamines protected with photolabile carbamates has been synthesized by reac- tion between the corresponding ,-diamines and either o-nitrobenzyl or 1-(2-nitrophenyl)ethyl phenyl carbonate.

Facile Synthesis of o-Nitrobenzylcarbamate and 1-(2-Nitrophenyl ethyl) Carbamate Protected α,ω-Diamines