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CuKα radiation ( = 1.5418 Å) using a Siemens D5005 diffractometer. The XRD data were collected between 2θ = 5 and 80° (in steps of 2° min -1 ). Transmission electron microscopy (TEM) images were obtained using a Tecnai FEI G20 operated at 200 kV. Samples were prepared by drop casting an alcoholic suspension of nanomaterial in carbon coated copper grid. 1 H nuclear magnetic resonance (NMR) spectra were recorded at 300 MHz instrument with chemical shifts reported relative to tetramethylsilane (TMS), with CDCl3 as solvent. Enantiomeric excesses (ee) were determined by gas chromatography (GC) analysis using a TRACETM 1310 Thermo Scientific TM chromatograph with a beta cyclodextrin capillary column. The lowresolution mass spectra (LRMS) were recorded on a Shimadzu GCMS-QP2010 Plus mass-spectrometer. Optical rotations were performed on A.Krüss Optronic automatic polarimeter P3000 (λ 589 nm) using a cell with a path length of 50 mm. All racemic amide products were prepared by reaction with Ac2O in the presence of Et3N, using CH2Cl2 as the solvent, following the procedure described in “General procedure for racemization of (S)-1-phenylethylamine” section.

Preparation, Characterization and Catalytic Activity of Palladium Catalyst Supported on MgCO3 for Dynamic Kinetic Resolution of Amines