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Three- and five-quantum  17 O MAS NMR experiments are used to resolve fully the three crystallographically distinct oxygen species in forsterite (Mg 2 SiO 4 ). The chemical shift and quadrupolar parameters extracted from these spectra are compared with the literature values obtained using conventional  17 O MAS and dynamic-angle-spinning (DAS) NMR.

Three- and five-quantum 17 O MAS NMR of forsterite Mg 2 SiO 4