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Adhesion and crack formation of coating films prepared from methyltriethoxysilane (MTES) on stainless steel sheets (SUS) after a thermal shock test were studied and their relation to a structure change of the films was discussed. Peeling-off caused by crack formation of the coating films prepared from MTES was observed after the thermal shock test at temperatures higher than 450°C. It was found that these damages were brought about by densification with the thermal decomposition of CH3 groups in the MTES-derived films and also by difference in thermal expansion coefficient between coating film and SUS substrate. For the purpose of the improvement of the above properties, composite coatings containing various oxide powders, such as SiO2, Al2O3, ZrSiO4, MnO2 and Fe2O3, were made. Adhesion after the thermal shock test in the composite films with any of these powders was considerably improved due to the reinforcement by the added powders, the expansion coefficient of which was close to that of SUS.

Coatings of Composite Films Prepared from CH3Si(OC2H5)3 and Various Oxide Powders on Stainless Steel Sheets.