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Metabolomics can be used for the analysis of volatile organic compounds (VOCs), which can be found in biological fluids and are synthesized in biological systems in normal metabolisms or in diseases, indicating their potentiality to be used as biomarkers. In this work, urine and blood serum samples from healthy individuals were used to optimize the sample preparation method by headspace solid phase microextraction (HS-SPME) followed by gas chromatography coupled to mass spectrometry (GC-MS).

Analysis of the metabolomic profile of volatile organic compounds in biological fluids by GC-MS