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Dinuclear nickel(II) complex, [Ni2{O2CC(CH3)3}4(OH2){HO2CC(CH3)3}4] (1), was synthesized and characterized by elemental analysis, IR and UV-Vis-NIR spectroscopy, and temperature dependence of magnetic susceptibilities (4.5—300 K). Single-crystal X-ray crystallography revealed a dinuclear core with μ-aqua and di-μpivalato bridges having monodentate pivalato and monodentate pivalic acid molecules. Magnetic data analysis showed a ferromagnetic interactions between the two nickel atoms with g = 2.251, J = 2.78 cm, D = 3.75 cm, and tip = 184 x 10 cm mol; g = 2.253, J = 2.73 cm, D = –3.26 cm, and tip = 176 x 10 cm mol.

Dinuclear Nickel(II) Pivalate with Μ-Aqua and Di-Μ-Pivalato Bridges Showing a Ferromagnetic Interaction