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The large volume of industrially-produced oily wastewater has resulted in alarming levels of environmental pollution and resource usage problems. A wide range of conventional and emerging approaches has been established that can effectively reduce these pollutants to an acceptable level so that the treated wastewater can be discharged for reuse [1]. Oily wastewater pollution generally consists of the following aspects: affects drinking water and groundwater resources, endangers aquatic resources, endangers human health, pollutes the atmosphere, affects crop production, destroys the natural landscape, all occurring most likely because of the accumulation of this oily residue [2]. Membrane filtration is a highly desirable solution for removing oil from oily wastewater because of its advantages of energy efficiency, easy processing, and low maintenance costs [3]. Membranes consist of a barrier that separates two phases and which totally or partially restricts the transport of one or several chemical species in the phases [4]. Synthetic membranes can be fabricated from polymeric materials as well as ceramic materials. Membrane restricts the transport of particulate matter, colloidal and chemical species dissolved in organic solvents or water [4]. Selective transport is performed based on the differences in the physical and/ or chemical characteristics of the components permeating through the membrane. In recent years, membrane processes are widely used in the textile, pharmaceutical, cellulose, semiconductor, leather tanning, mining, electroplating, dairy, food processing and beverage industries [5, 6]. The processes of separation by membranes have advantages due to their low costs in long-term operational terms due to their chemical and thermal stability, energy savings and selectivity [7]. The processes that utilize membranes in the separation are effective compared to conventional distillation Influence of the methodology on the formation of zeolite membranes MCM-22 for the oil/water emulsion separation