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The crystal structure of [Cu( Him ) 2 (CO 3 )]·H 2 O, determined from conventional X-ray powder diffraction methods, allowed to clarify, on the basis of a structural interpretation of the chemical transformation, the role of the title compound in the formation of the blue phase of Cu(im) 2  [Cu(Him) 2 (CO 3 )]·H 2 O is triclinic,  P 1̅;  a  = 8.8565(7),  b  = 8.9579(5),  c  = 8.3705(6) Å,  α  = 105.728(4)°,  β  = 105.318(3)°,  γ  = 114.369(4)°; final  R wp  ,  R p   and  R F   agreement factors, for 4700 data collected in the 11–105° range, are 0.053, 0.036 and 0.078, respectively.

[Cu(imidazole) 2 (CO 3 )]⋅H 2 O: an intermediate in the formation of the copper bis-imidazolate polymer (blue phase)