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Synthesis and properties of two iridium(III) complexes ( 1  and  2 ) isolated from the same system upon change in organic solvent, are presented.  1  is a mononuclear compound with two bidentate oxime ligands linked by a strong intramolecular hydrogen bond and with two chlorido ligands in the central Ir 3+  ion coordination sphere.  2  is a binuclear centrosymmetric anionic complex with two Ir 3+  ions double-bridged by chlorido ligands and three terminal chlorido ligands further coordinated to two sodium cations to form a characteristic aggregate with acetonitrile molecules completing coordination spheres of the metal ions. Both  1  and  2  may help to develop a route to products analogous to Co(II) SMMs (Single Molecule Magnets) also as starting materials.

Iridium(III) products isolated in a reaction of IrCl 3 with phenyl 2-pyridyl ketoxime