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The tin atom in Me 2 Sn(phen)Cl 2  is located on a crystallographic site of symmetry  m2m  and exists within a distorted octahedral geometry defined by a C 2 Cl 2 N 2  donor set with the tin-bound methyl groups occupying  trans -positions. A two-dimensional array stabilised by C–H · · · Cl interactions is established in the crystal structure. Crystal data for Me 2 Sn(phen)Cl 2 : C 14 H 14 Cl 2 N 2 Sn,  M  = 399.90, orthorhombic space group  Cmcm ,  a  = 11.359(2),  b  = 18.910(5),  c  = 7.536(2) Å,  V  = 1618.7(11) Å 3 ,  Z  = 8,  R  = 0.073.

Crystal and molecular structure of dichloro(1,10-phenanthroline)dimethyltin(IV), Me 2 Sn(1,10-phenanthroline)Cl 2 , determined by neutron diffraction