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The dicyanamido diethelenetriamine copper (II) compound, C 8 H 13 CuN 9  (I), has been synthesized, and structurally characterized independently using X-ray powder- and single-crystal diffraction data. The direct methods program package EXPO-2004 has been used for structure solution from laboratory powder diffraction data. Intermolecular N—H···N hydrogen bonds in (I) generate R 2  2 (16) rings, which are fused forming molecular columns propagating along the [100] direction. Further linking of parallel columns through N—H···N hydrogen bonds results into a three-dimensional supramolecular network.

A comparative study of crystal structure of a Cu(II) dicyanamide compound determined independently from X-ray powder- and single-crystal analyses