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Crystals of thallium dihydrogendiphosphate Tl 2  Me (H 2 P 2 O 7 ) 2  · 2 H 2 O ( Me  = Mg  (1) , Mn  (2),  Co  (3) , Ni  (4)  and Zn  (5) ), have been synthesized and analyzed by powder X-ray diffractometry (Mg phase) and single crystal X-ray diffractometry (other phases). They resulted to be isostructural within triclinic group  P -1, with the following unit-cell parameters:  a  = 6.9620(1),  b  = 7.3635(1),  c  = 7.7713(1) Å,  α  = 81.8014(5),  β  = 70.8597(6),  γ  = 86.1373(7)°,  V  = 372.44(8) Å 3  (1) ;  a  = 6.9577(6),  b  = 7.4745(6),  c  = 7.8248(7) Å,  α  = 80.723(2),  β  = 71.912(1),  γ  = 85.661(1)°,  V  = 381.62(6) Å 3  (2) ;  a  = 6.9767(7),  b  = 7.3634(7),  c  = 7.7690(7) Å,  α  = 81.421(2),  β  = 71.114(2),  γ  = 86.424(2)°,  V  = 373.36(6) Å 3  (3) ;  a  = 6.9658(7),  b  = 7.3079(7),  c  = 7.7016(7) Å,  α  = 81.801(2),  β  = 71.185(2),  γ  = 86.528(2)°,  V  = 367.27(6) Å 3  (4)  and  a  = 6.9628(7),  b  = 7.3625(7),  c  = 7.7401(8) Å,  α  = 81.590(2),  β  = 71.441(2),  γ  = 86.323(2)°,  V  = 372.04(6) Å 3  (5) .

zeitschrift für kristallographie - crystalline materials

New thallium diphosphates Tl 2  Me (H 2 P 2 O 7 ) 2  · 2 H 2 O,  Me  = Mg, Mn, Co, Ni and Zn. Synthesis, single crystal X-ray structures and powder X-ray structure of the Mg phase