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Bisferrocenium hexadecaiodide (bis-dicyclopentadienyliron(III)hexadecaiodide) [Cp 2 Fe] 2 I 16  (Cp =  η  5 -C 5 H 5 ) has been prepared in acetonitrile by reaction of ferrocenium triiodide and excess iodine in the molar ratio of 1:14. It crystallizes at 293 K in the triclinic space group  P [unk] with  a  = 11.558(3) Å,  b  = 11.877(3) Å,  c  = 18.754(6) Å,  α  = 102.13(2)°,  β  = 100.99(2)°,  γ  = 107.72(3)°,  V  = 2306(1) Å 3  and  Z  = 2. The crystal structure has been refined by full matrix least-squares procedures to  R ( F ) = 0.0546 for 5525 reflections. Bisferrocenium hexadecaiodide contains nets of hexadecaiodide units forming channels along [110] filled by columns of disordered complex cations (Cp 2 Fe) + .

Darstellung und Kristallstruktur von Bisferroceniumhexadecaiodid, [Cp 2 Fe] 2 I 16 1