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Actinide cation–cation complexes in aqueous solution have long been a subject of interest. Since the former work of Sullivan  et al. , several complexes of this type have been discovered, all of them involving an actinide(V) oxocation and either another actinide oxocation or a transition metal cation. Although many studies have been devoted to the structure analysis of such complexes, they have been lacking evidences for the definition of a structural model. In this report, EXAFS spectroscopy has been tentatively used, considering two possible interaction modes: bridging or linear Np–Np interaction.

Np(V) cation–cation interactions. A new contribution from EXAFS spectroscopy?