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Stabilization of recoil  56 Mn in mixed crystals of MnSO 4 KClO 4  was studied with especial emphasis on isothermal annealing of neutron irradiated target. The results showed that  * MnO 4  -  yield (%) varies linearly with the increase in perchlorate concentration from 0.100 to 0.500 mol fraction, reaching a maximum value of (89.0 ± 1.1)%. However, the value of intercept ( P  0 ) obtained was (63.0 ± 1.2)%. Isothermal annealing of  56 Mn in the present mixed crystal (MnSO 4 KClO 4 ) of the two molar concentrations ( i.e. , 0.100 and 0.500 mol fraction) of perchlorate was studied at different temperatures for a desired length of time. The retention values increased with increasing temperature and time of annealing for both the samples. The values found for the two concentrations were (67.0 ± 1.0)% and (89.0 ± 1.1)%, respectively, at room temperature. Retention value increased gradually in the beginning but slowed down with a lapse of time and finally attained saturation within about 20 min of heating at 373 K in both cases. Limiting saturations were found to be (86.0 ± 1.0)% (max) for 0.100 molar concentration and (96.0 ± 0.8)% (max) for 0.500 molar concentration.

Chemical stabilization of recoil 56 Mn in MnSO 4 -KClO 4 mixed crystals following ( n , γ) process