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We produced  229 Th in the nuclear reaction  232 Th(γ,  p 2 n )  229 Ac, followed by disintegration to  229m,g Th. The  229m Th α-decay was searched for. Alpha-particle events of energy between 4.93 MeV and 5.05 MeV were observed in the separated thorium sample of β-decay products from an actinium source highly purified from the  232 Th + γ reaction products. The energies of the α-particles coincide with those expected for  229m Th.

Search for α-decay of 229m Th produced from 229 Ac β-decay following 232 Th(γ, p 2 n ) reaction