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C 16 H 26 N 2 O 7 P 2 , monoclinic, C12/c1 (No. 15), a = 32.53(1) A, b = 8.415(2) A, c = 7.792(4) A, β = 92.18(3)°, V = 2131.4 A 3 , Z = 4, R gt (F) = 0.071, wR ref (F) = 0.077, T = 296K.

Crystal structure of bis(3,5-dimethylanilinium) dihydrogenodiphosphate, (C 8 H 12 N) 2 H 2 P 2 O 7