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The donor-free potassium silanide K[SiPh 3 ] was prepared by the reaction of hexaphenyldisilane, Ph 3 Si–SiPh 3 , with potassium metal in benzene at room temperature. The solid-state structure, determined by powder X-ray diffraction consists of {K[SiPh 3 ]} 2  units, which interact with adjacent dimers to form an infinite chain along the crystallographic  c  axis (orthorhombic, space group  Cmc 2 1 ,  Z =4). The structure features short contacts between the π system of the phenyl rings and the potassium atoms of neighbouring K[SiPh 3 ] units.

Synthesis and structure of the donor-free potassium silanide K[SiPh 3 ]