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Interaction of (NH 4 ) 6 Mo 7 O 24 ·4H 2 O with tris-(3,5-di- tert -butyl-2-hydroxy-benzylidene)triaminoguanidinium chloride [H 6   t  Bu 6 L]Cl in DMF-H 2 O resulted in isolation of a neutral dinuclear Mo(VI) complex [Mo 2 O 4 (OH 2 )(DMF)(H  t  Bu 6 L)]·3DMF. The  C  3 -symmetric-type ligand H  t  Bu 6 L is coordinated to two  cis -{MoO 2 } 2+  moieties via phenolic-oxygen, guanidine nitrogen and azomethine nitrogen atoms, and the remaining sixth coordination sites of the molybdenum centers are occupied by the oxygen atoms from the solvent molecules.

zeitschrift für naturforschung b

A dinuclear molybdenum(VI) complex with a triaminoguanidine ligand: synthesis and structure of [Mo 2 O 4 (OH 2 )(DMF)(H  t  Bu 6 L)]·3DMF ([H 6   t  Bu 6 L]Cl=tris(3,5-di- tert -butyl-2-hydroxybenzylidene)-triaminoguanidinium chloride)