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β -Y(BO 2 ) 3  was synthesized in a Walker-type multianvil module at 5.9 GPa/1000°C. The crystal structure has been elucidated through single-crystal X-ray diffraction.  β -Y(BO 2 ) 3  crystallizes in the orthorhombic space group  Pnma  (no. 62) with the lattice parameters  a  = 15.886(2),  b  = 7.3860(6), and  c  = 12.2119(9) Å. Its crystal structure will be discussed in the context of the isotypic lanthanide borates  β - Ln (BO 2 ) 3  ( Ln  = Nd, Sm, Gd–Lu).

β -Y(BO 2 ) 3 – a new member of the β - Ln (BO 2 ) 3 ( Ln =Nd, Sm, Gd–Lu) structure family