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The praseodymium borate-nitrate Pr[B 5 O 8 (OH)(H 2 O) 0.87 ]NO 3 ·2H 2 O was obtained in a hydrothermal synthesis. It crystallizes monoclinically in the space group  P 2 1 / n  (no. 14) with four formula units ( Z =4) and unit cell parameters of  a =641.9(3),  b =1551.8(7),  c =1068.4(5) pm, with  β =90.54(2)° yielding  V =1.0643(8) nm 3 . The defect variant constitutes the missing member in the series of isostructural, early rare earth borate-nitrates of the composition  RE [B 5 O 8 (OH)(H 2 O)  x  ]NO 3 ·2H 2 O [ RE =La ( x =0; 1), Ce ( x =1), Nd ( x =0.85), Sm ( x =0)]. In addition to powder and single-crystal X-ray diffraction data, the novel borate-nitrate was characterized through IR and Raman spectroscopy.

Hydrothermal synthesis and characterization of the praseodymium borate-nitrate Pr[B 5 O 8 (OH)(H 2 O) 0.87 ]NO 3 ·2H 2 O