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The crystal structure of NH 4 [C(CN) 3 ] has been determined via X-ray single-crystal methods at 203(2) K corroborating earlier results. Additionally, the hydrogen positions have been determined and the Raman spectrum of the title compound recorded on single crystals. The spectroscopic results are compared to those for related compounds.

Complete X-ray single-crystal structure determination and Raman spectrum of NH 4 [C(CN) 3 ]