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Treatment of [Ru(acac) 3 ] (acac − =acetylacetonate) with (2,4,5-Me 3 C 6 H 2 )MgBr, followed by column chromatography in air, afforded the homoleptic tetraaryl-ruthenium(IV) complex [Ru(2,4,5-Me 3 C 6 H 2 ) 4 ] ( 1 ) in moderate yield. The product was characterized by proton NMR spectroscopy and microanalyses. Its crystal structure has also been established by X-ray crystallography.

Synthesis and crystal structure of a new homoleptic tetraarylruthenium(IV) complex Ru(2,4,5-Me 3 C 6 H 2 ) 4