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Orthorhombic In 3 B 5 O 12  was synthesized in a Walker-type multianvil apparatus under high-pressure/high-temperature conditions of 12.2 GPa and 1500°C. Its structure is isotypic to the rare earth analogs  RE  3 B 5 O 12  ( RE =Sc, Er–Lu). In the field of indium borate chemistry, In 3 B 5 O 12  is the third known ternary indium borate besides InBO 3  and InB 5 O 9 . The crystal structure of In 3 B 5 O 12  has been determined via single-crystal X-ray diffraction data collected at room temperature. It crystallizes in the orthorhombic space group  Pmna  with the lattice parameters  a =12.570(2),  b =4.5141(4),  c =12.397(2) Å, and  V =703.4(2) Å 3 . IR and Raman bands of In 3 B 5 O 12  were theoretically determined and assigned to experimentally recorded spectra.

High-pressure synthesis and crystal structure of In 3 B 5 O 12