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A mixed-valence Cu(I)/Cu(II) coordination polymer, namely, [Cu 2 (L)(1,3-BDC)]  n   ( 1 ), has been synthesized under hydrothermal conditions (HL = 2-(2-fluorophenyl)-1 H -imidazo[4,5- f ][1,10]phenanthroline and 1,3-H 2 BDC = 1,3-benzenedicarboxylic acid). Its structure has been determined by single crystal X-ray diffraction analysis and powder X-ray diffraction. The crystals are the monoclinic space group  P 2 1 / c  with  a  = 10.686(4),  b  = 17.376(8),  c  = 11.759(4) Å,  β  = 92.072(14)°, C 27 H 14 Cu 2 FN 4 O 4 ,  M  r  = 604.50,  V  = 2182.1(15) Å 3 ,  Z  = 4,  D  calcd.  = 1.84 g cm –3 ,  R  = 0.0588 and  wR  = 0.1202 (all data). In complex  1 , the mixed-valence Cu(I)/Cu(II) atoms are linked by L and 1,3-BDC to give a rare 3D (3,3,4)-connected (4.7.9)(7.8.9)(4.7.8.9 3 ) framework. The temperature-dependent magnetic susceptibility of  1  was investigated in the temperature range of 2–300 K.

zeitschrift für naturforschung b

A 3D mixed-valence Cu(I)/Cu(II) coordination polymer constructed by 2-(2-fluorophenyl)-1 H -imidazo[4,5- f ][1,10]phenanthroline and 1,3-benzenedicarboxylate